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분체공학, 유동충, 고분자, 재료(무기, 유기) : LiNiO2의 합성 최적조건 확립 및 과량의 리튬함량과 Al 도핑이 전기화학적 특성에 미치는 영향
박기수 ( Ki Soo Park ),조명훈 ( Myung Hun Cho ),박상호 ( Sang Ho Park ),선양국 ( Yang Kook Sun ),이윤성 ( Yun Sung Lee ),마사키요시오 ( Masaki Yoshio ),남기석 ( Kee Suk Nahm ) 한국화학공학회 2003 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.41 No.1
LiNiO_2, Li_(1+x)NiO_2(x=0.00-0.05) and LiAl_yNi_(1-y)O_2 (y=0.00-0.3) powers were synthesized using a sol-gel method. To synthesize LiNiO_2 with a good electrochemical performance, the experiments were carried out as function of the molar ratio of adipic acid to total metal ions, excess Li content, and Al doping. The synthesized LiNiO_2 powders showed a good crystal quality when the molar ratio of adipic acid to total metal ions was 1.0. The analysis of gas composition evolved during the decomposition of gel precursors revealed that oxygen played an important role in improving the crystal quality of LiNiO_2 powders. All the prepared Li_(1+x)NiO_2 powders had a typical LiNiO_2 layered structure, but the electrochemical performance was degraded with the increasing the lithium content. Al-doped LiAl_yNi_(1-y)O_2 powdwers were better than LiNiO_2 powders in cyclicality though it showed a low initial discharge capacity. The Al doped LiAl_yNi_(1-y)O_2 powders presented a good electrochemical performance even at higher temperatures.
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졸-겔법에 의해 제조된 LiMPO<sub>4</sub>(M = Fe, Mn) 양극 활물질의 전기화학적 특성
김재광,백동호,신용조,안주현,서양곤,김지수,윤석준,조명훈,Kim, Jae-Kwang,Baek, Dong-Ho,Shin, Yong-Jo,Ahn, Jou-Hyeon,Seo, Yang-Gon,Kim, Chi-Su,Yoon, Seok-Jun,Cho, Myung-Hun 한국전기화학회 2008 한국전기화학회지 Vol.11 No.2
Carbon-coated $LiFePO_4$ and $LiMn_{0.4}Fe_{0.6}PO_4$ cathode materials for lithium batteries were synthesized by a sol-gel method. X-ray diffraction and scanning electron microscopy data showed that the cathode materials are pure crystalline and are surrounded by porous carbon. The initial discharge capacities of $LiFePO_4$ and $LiMn_{0.4}Fe_{0.6}PO_4$ with the liquid electrolyte of 1M $LiPF_6$ in EC/DMC are 132 mAh/g and 145 mAh/g, respectively, at current density of 0.1 C-rate. $LiFePO_4$ and $LiMn_{0.4}Fe_{0.6}PO_4$ with an electrospun polymer-based electrolyte exhibit initial discharge capacities of 114 and 130 mAh/g at 0.1 C-rate at room temperature, respectively.
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